Characterization of Dyestuffs and Metals from Selected 16-17th-Century Ottoman Silk Brocades by RP-HPLC-DAD and FESEM-EDX

Karadag R., Torgan E., Taskopru T., Yildiz Y.

JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, cilt.38, sa.5, ss.591-599, 2015 (SCI-Expanded) identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 38 Sayı: 5
  • Basım Tarihi: 2015
  • Doi Numarası: 10.1080/10826076.2014.922476
  • Dergi Adı: JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.591-599
  • Anahtar Kelimeler: dyestuff, Ottoman silk brocade, metal thread, FESEM-EDX, cultural heritage, HPLC-DAD, PERFORMANCE LIQUID-CHROMATOGRAPHY, DACTYLOPIUS-COCCUS COSTA, DIODE-ARRAY DETECTION, RESEDA-LUTEOLA L., RED NATURAL DYES, TEXTILES, IDENTIFICATION, PIGMENTS, THREADS, WELD
  • Marmara Üniversitesi Adresli: Evet

Özet

In this study, the analysis of dyestuff and metal thread samples present in the 16-17th-century Ottoman silk textile samples were performed by HPLC-DAD (high-performance liquid chromatography coupled with diode array detection) and FESEM-EDX (field emission scanning electron microscopy with energy dispersion spectroscopy). HPLC-DAD was used for the identification of dyestuffs in different plants and insects such as weld, dyer's oak, walloon oak, woad, indigo, madder, young fustic, and cochineal. Silk yarns with yellow, blue, orange, brown, red, and green colors were selected for the analysis. One of the most useful procedures for fast and simple determination of specific metals of interest is FESEM-EDX. This is a simple method that provides information on chemical composition of sample surfaces and chemical analysis of metal threads.